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11 g b v y W { C w A j E t B n j A nj y c EAC @Angel i EMI j 2,100 Ã R h @ iNo C 327 B G j t X L /. XXVII (11 g), 125 ml XIX, 42 g anhyd K2CO3, and 05 g Cubronze powder stirred and refluxed under dry N until CO2 evolution was complete (125 hrs), the mixt filtered, the filter cake washed with XIX, the combined filtrate and washings poured into 1 l cold H2O, and the mixt allowed to stand 2 hrs at room temp gave 06 g. 1=a =J;N" J ;.
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J SN a#S";WN 8 7 ;. XRAY LINE BROADENING FROM FILED ALUMINIUM AND WOLFRAM* G K WILLIAMSONf and W H HALLf Methods ot analysis previously used in the interpretation of line broadening are discussed and are shown to be inadequate;. ¼†\ MOBI ýéúïn> ÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿÿ^ R" aXPÿÿÿÿÿÿÿÿ h j i ÿÿÿÿÿÿÿÿÿÿÿÿ.
@ s A g } g } g A N b i ԁA F A A s N A F A I W A j A @ ɉ ς B. A 500mL, threenecked, roundbottomed flask is equipped with a mechanical stirrer, nitrogen inlet adapter, and 150mL pressureequalizing dropping funnel fitted with a rubber septum (Note 1)The flask is charged with 70 mL of dry tetrahydrofuran (Note 2) and 159 mL (0075 mol) of 1,1,1,3,3,3hexamethyldisilazane (Note 3), and then cooled in an icewater bath while 2 mL (0072 mol). More reliable methods being outlined.
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